DH677.3 structural data collection and refinement statistics

  • a Rmerge = ∑|I − |/∑I, where I is the observed intensity and the average intensity obtained from multiple observations of symmetry-related reflections after rejections.

  • b Rpim, defined in reference 1.

  • c CC1/2, defined by Karplus and Diederichs (56).

  • d R = ∑║Fo|− | Fc║/∑|Fo |, where Fo and Fc are the observed and calculated structure factors, respectively.

  • e Rfree, as defined by Brünger (57).

  • f RMSD = Root mean square deviation

  • g Calculated with MolProbity.

  • h Values in parentheses are for the highest-resolution shell.